Analytical Methods Lab (B.Sc Chemistry)

Organic preparations, gravimetric estimations and thermochemical and electrochemical experiments.

6 महीनेअवधि 4Chapters17टॉपिक

सिलेबस · पाठ्यक्रम

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01Organic Preparations 5 टॉपिक
  1. Aspirin from salicylic acid
  2. Acetanilide from aniline
  3. p-Bromoacetanilide from acetanilide
  4. m-Dinitrobenzene from nitrobenzene
  5. Recrystallisation, yield and melting point
02Gravimetric Analysis 4 टॉपिक
  1. Barium as BaSO4
  2. Nickel as Ni-DMG
  3. Iron as Fe2O3
  4. Digestion, filtration and ignition to constant weight
03Thermochemical Experiments 4 टॉपिक
  1. Water equivalent of calorimeter
  2. Enthalpy of neutralisation
  3. Enthalpy of solution
  4. Enthalpy of hydration of CuSO4
04Electrochemical Experiments 4 टॉपिक
  1. EMF of Daniell cell
  2. Electrode potential of Zn and Cu electrodes
  3. Verification of Ostwald's dilution law
  4. Potentiometric determination of a redox end point

परिचय

आप यह कर पाएँगे

  • Prepare simple organic compounds, recrystallise them and report yield and melting point
  • Carry out gravimetric estimations with correct digestion, filtration and ignition
  • Determine enthalpies of neutralisation and solution with a calorimeter
  • Measure EMF and electrode potentials of cells
  • Write a complete practical record and face the viva

यह किसके लिए है

  • B.Sc Chemistry students of Semester 6 (UP State Universities, NEP 2020)
  • Students preparing for the B.Sc Chemistry practical examination and viva

आपको क्या चाहिए

  • Theory of Organic Synthesis-B and Chemical Energetics
  • Lab coat, goggles and fume hood use

सवाल

Which syllabus does this lab course follow?

It follows the B.Sc Chemistry Semester 6 syllabus of the UP State Universities (NEP 2020 common minimum syllabus). Where your own university's syllabus differs, the centre follows your university syllabus.

How are students assessed at the centre?

The trainer watches each experiment and marks it on a rubric (set-up, observations, calculation and viva); viva-style questions revise the theory behind the experiments.

Will this help in the semester examination?

Yes. The experiments match the university practical examination, including the record file and viva.

Download the syllabus (PDF)

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